Please use this identifier to cite or link to this item:
https://hdl.handle.net/20.500.14279/2031
Title: | Bis(4,6-diaminopyrimidin-2-yl) disulfide dimethyl sufoxide disolvate |
Authors: | Shakhatreh, Saleh K. Akrivos, Pericles D. Gdaniec, Maria Papastavrou, Evridiki |
Major Field of Science: | Natural Sciences |
Field Category: | Chemical Sciences |
Keywords: | Single-crystal X-ray study |
Issue Date: | 2008 |
Source: | Acta Crystallographica Section E: Crystallographic Communications, 2008, vol. 64, iss. 9, pp. o1724 |
Volume: | 64 |
Issue: | 9 |
Start page: | o1724 |
Journal: | Acta Crystallographica Section E: Crystallographic Communications |
Abstract: | The title compound, C8H10N8S2·2C2H6SO, was obtained unintentionally during an attempt to prepare a thiol-ate derivative of trimethyl-tin. The complete disulfide mol-ecule is generated by twofold rotation symmetry and the C - S - S - C torsion angle around the S - S bond is -85.70 (10)°. The mol-ecules are connected via N - H⋯N hydrogen bonds into strongly corrugated layers parallel to (001), generating an R 2 2(8) motif. The solvent mol-ecule, which exhibits minor disorder of its S atom [site occupancies = 0.9591 (18) and 0.0409 (18)], is linked to this layer via a pair of N - H⋯O inter-actions. |
URI: | https://hdl.handle.net/20.500.14279/2031 |
ISSN: | 20569890 |
DOI: | 10.1107/S160053680802480X |
Rights: | © International Union of Crystallography |
Type: | Article |
Affiliation : | Aristotle University of Thessaloniki |
Publication Type: | Peer Reviewed |
Appears in Collections: | Άρθρα/Articles |
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