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  4. Does microstructure matter for statistical nanoindentation techniques?
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Does microstructure matter for statistical nanoindentation techniques?

Journal
Cement and Concrete Composites
Date Issued
January 2010
Author(s)
Constantinides, Georgios  
Ulm, Franz Josef  
Vandamme, Matthieu  
Jennings, Hamlin M.  
Vanzo, James  
Bentivegna, Michelle  
Krakowiak, Konrad J.  
Bobko, Christopher P.  
Vliet, Krystyn J Van  
DOI
10.1016/j.cemconcomp.2009.08.007
Abstract
In their paper, Trtik et al. (2009) identify spurious peaks in the application of statistical nanoindentation technique as a critical obstacle for mechanical phase identification. In this discussion, we show that Trtik et al.'s finding is a consequence of an unrealistic virtual 3-D checkerboard microstructure considered by the authors. These peaks are not a general feature of indentation on multiphase materials, nor can the presence of such peaks be attributed to an intrinsic shortcoming of the grid-indentation technique. We also show that the authors' assertion of the absence of homogeneous material regions extending beyond 3 μm in cementitious materials is groundless.
Subjects

Microstructure

Statistical methods

Cement composites

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